P,P-双(4-甲基苯基)-氯化膦 氯二对甲苯基膦合成路线 (共 10 条)
反应条件
phosphorus trichoride in toluene; benzene T=0 - 10°C; 0.5 h;
参考文献
Narsireddy, Meda; Yamamoto, Yoshinori
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9698 - 9709
反应条件
1: With pyridine in diethyl ether 2 h; Heating; 2: With hydrogenchloride in diethyl ether T=20°C; 10 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 129, # 25 p. 7734 - 7735
反应条件
(i) Mg, THF, (ii) Et2NPCl2; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 100, p. 7304 - 7311
反应条件
aluminium trichloride; phosphorus trichoride T=140 - 150°C; 5 h;
参考文献
Kormachev, V. V.; Vasil'eva, T. V.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 1 p. 224 - 225,199 - 200
参考文献
Justus Liebigs Annalen der Chemie, , vol. 315, p. 68
反应条件
N,N-diethylaniline in diethyl ether; water
参考文献
Quin,L.D.; Anderson,H.G.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1206 - 1209
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
反应条件
1: LiAlH4 2: O2 View Scheme
参考文献
Strecker,R.A. et al.
Journal of the American Chemical Society, 1973 , vol. 95, p. 210 - 214
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 95, p. 210 - 214
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831