3,5-二硝基-4-羟基苯甲酸合成路线 （共 47 条）
反应条件
in methanol; thionyl chloride
参考文献
The Rockefeller University; Alteon Inc.
Patent: US5514676 A1, 1996 ;
参考文献
Nevole
Chemische Berichte, 1944 , vol. 77/79, p. 61,63
反应条件
(i) SOCl2, toluene, (ii) aq. NH3; Multistep reaction;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 6, p. 559 - 564,556 - 561
反应条件
in conc. nitric acid; sulfuric acid; water
参考文献
HWANG, Kuen Yuan; Tu, An Pang; Wu, Sheng Yen; Chen, Gai Chi; Huang, Ching Jui; Wang, Jen Fu
Patent: US2011/172324 A1, 2011 ;
反应条件
sodium hydroxide in water; acetonitrile
T=25°C; in the presence of cetyltrimethylammonium chloride; other surfactants; var. conc. of NaOH; Rate constant;
参考文献
Cipiciani, Antonio; Primieri, Stefania
Australian Journal of Chemistry, 1991 , vol. 44, # 10 p. 1505 - 1509
反应条件
sulfuric acid; nitric acid
T=0°C; 3 h;
参考文献
Hankovszky, H. Olga; Hideg, Kalman; Jerkovich, Gyula
Synthesis, 1989 , # 7 p. 526 - 529
反应条件
potassium metabisulfite; nitric acid
Diazotization.nachfolgend Behandeln mit Kupfer(II)-sulfat;
参考文献
Elion
Recueil des Travaux Chimiques des Pays-Bas, 1923 , vol. 42, p. 151,153,164,168
Recueil des Travaux Chimiques des Pays-Bas, 1924 , vol. 43, p. 867
反应条件
nitric acid; acetic acid
T=60°C;
参考文献
Biehringer; Borsum
Chemische Berichte, 1915 , vol. 48, p. 1316
参考文献
Goldschmiedt; Zerner
Monatshefte fuer Chemie, 1910 , vol. 31, p. 464,468
参考文献
Goldstein; Giddey
Helvetica Chimica Acta, 1954 , vol. 37, p. 2083,2086
