(1-羟基乙基)膦酸二甲基酯合成路线 (共 9 条)
反应条件
sodium methylate in methanol; diethyl ether T=-35°C; 0.166667 h;
参考文献
Li, Yong-Fu; Hammerschmidt, Friedrich
Tetrahedron: Asymmetry, 1993 , vol. 4, # 1 p. 109 - 120
反应条件
triethylamine in diethyl ether
参考文献
Nurtdinov,S.Kh. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, p. 2446 - 2452,2159 - 2165
反应条件
1: T=25°C; 0.166667 h; 2: With aluminum oxide; potassium fluoride 0.5 h;
参考文献
Nagar, Mitesh; Lietzan, Adam D.; St. Maurice, Martin; Bearne, Stephen L.
Biochemistry, 2014 , vol. 53, # 7 p. 1169 - 1178
参考文献
Abramow; Semenowa
Sb. Statei Obshch. Khim., 1953 , p. 393,395
Chem.Abstr., 1955 , p. 838
反应条件
organic base in chloroform T=20 - 40°C; 5 h;
参考文献
Wang, Tao; Hong, Wu He
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 10 p. 2081 - 2089
反应条件
hydrogenchloride
T=40 - 45°C; 1 h;
参考文献
Gazizov, M. B.; Khairullin, R. A.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 7 p. 1493 - 1504,1332 - 1341
反应条件
triethylamine in tetrahydrofuran
T=39 - 41°C;
参考文献
Gazizov, M. B.; Shergina, I. I.; Krasil'nikova, E. A.; Baturova, O. V.; Akhmetshina, F. R.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 12 p. 2792 - 2793,2517
参考文献
Gazizov, M. B.; Khairullin, R. A.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 7 p. 1493 - 1504,1332 - 1341
反应条件
triethyl amine hydrochloride
参考文献
Eliseenkov,V.N. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 1760 - 1762
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, p. 1869 - 1871