(S)-(+)-2-甲基戊二酸二甲酯合成路线 (共 14 条)
反应条件
1: methyl (4S)-(2-methoxy-4-methylphenyl)pentanoate With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile T=20°C; 18 h; 2: With hydrogenchloride in water 3: diazomethane in diethyl ether
参考文献
Tetrahedron Asymmetry, , vol. 12, # 18 p. 2597 - 2604
反应条件
1: methyl (4S)-(4-methoxy-2-methylphenyl)pentanoate With ruthenium trichloride; sodium periodate in tetrachloromethane; acetonitrile T=20°C; 18 h; 2: diazomethane in diethyl ether
参考文献
Tanikawa, Shin; Ono, Machiko; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 5 p. 565 - 569
反应条件
1: methyl 4-(2'-methoxy-5'-methylphenyl)pentanoate With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile T=20°C; 18 h; 2: With hydrogenchloride in water 3: diazomethane in diethyl ether
参考文献
Tetrahedron Asymmetry, , vol. 12, # 18 p. 2597 - 2604
反应条件
1: methyl (4S)-(4-methoxy-2-methylphenyl)pentanoate; acetonitrile With ruthenium trichloride; sodium periodate T=20°C; 14 h; 2: diazomethane in diethyl ether T=0°C; 0.5 h; Further stages.;
参考文献
Nagumo, Shinji; Ono, Machiko; Kakimoto, Yo-ichiro; Furukawa, Tsuneo; Hisano, Tomoaki; Mizukami, Megumi; Kawahara, Norio; Akita, Hiroyuki
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6618 - 6622
反应条件
1: 4-(o-methoxy-p-tolyl)-pentanoic acid methyl ester; acetonitrile With ruthenium trichloride; sodium periodate T=20°C; 14 h; 2: diazomethane in diethyl ether T=0°C; 0.5 h; Further stages.;
参考文献
Nagumo, Shinji; Ono, Machiko; Kakimoto, Yo-ichiro; Furukawa, Tsuneo; Hisano, Tomoaki; Mizukami, Megumi; Kawahara, Norio; Akita, Hiroyuki
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6618 - 6622
反应条件
hydrogen; platinum(IV) oxide
参考文献
Tetrahedron, , vol. 26, p. 2825 - 2835
反应条件
hydrogen; platinum(IV) oxide
参考文献
Tetrahedron, , vol. 26, p. 2825 - 2835
参考文献
Journal of Natural Products, , vol. 71, # 4 p. 551 - 557
参考文献
Organic Letters, , vol. 12, # 13 p. 3022 - 3025
参考文献
Chemistry Letters, , # 7 p. 539 - 540
Chemistry Letters, , # 8 p. 741 - 742