(甲氧基-苯基甲基)苯合成路线 (共 143 条)
反应条件
1: benzyl methyl ether With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chlorobenzene
T=80°C; 1.5 h; Inert atmosphere;
2: phenyl-magnesium bromide in diethyl ether; chlorobenzene
T=0°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro; Li, Chao-Jun
Organic Letters, 2013 , vol. 15, # 14 p. 3650 - 3653
反应条件
1: benzyl methyl ether With 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene in 1,2-dichloro-ethane
T=80°C; 3 h; Inert atmosphere;
2: PhMgI in diethyl ether; 1,2-dichloro-ethane
T=-20°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro
Organic Letters, 2014 , vol. 16, # 7 p. 2042 - 2045
反应条件
methanol in acetonitrile
HeatingIrradiation; Further byproducts given;
参考文献
Albini, Angelo; Fasani, Elisa; Mella, Mariella
Journal of the American Chemical Society, 1986 , vol. 108, # 14 p. 4119 - 4125
反应条件
C16H18AuNP(1+)*F6Sb(1-) in toluene
T=120°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Chen, Yifeng; Chen, Ming; Liu, Yuanhong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 26 p. 6493 - 6497
反应条件
sodium methylate in methanol
T=70°C; 6.4 h; C-anode, C-cathode, 4.4 F/mol, constant current 0.5 A, undivided cell;
参考文献
Chiba, Toshiro; Okimoto, Mitsuhiro; Nagai, Hiroshi; Takata, Yoshiyuki
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2968 - 2972
反应条件
1: in methanol
T=50°C; 2 h;
2: With iron-copper nanoparticles in methanol
12 h; Reflux;
参考文献
Garcia, Marco A.; Garcia-Munoz, Angel; Pena, Josue A.; Trujillo-Reyes, Jessica; Morales-Luckie, Raul A.; Avalos-Borja, Miguel; Vilchis-Nestor, Alfredo R.; Sanchez-Mendieta, Victor; Corona, David; Cuevas-Yanez, Erick
Letters in Organic Chemistry, 2012 , vol. 9, # 1 p. 2 - 6
反应条件
in diethyl ether; toluene
T=25°C; 0.333333 h;
参考文献
Baruah, Mukulesh; Bols, Mikael
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 509 - 512
反应条件
in dichloromethane
T=20°C; 72 h;
参考文献
Grant, Jonathan W.; Smyth, Timothy P.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7965 - 7970
反应条件
methanol in acetonitrile
T=15°C; 16 h; Irradiation;
参考文献
Tomioka, Hideo; Inoue, Osamu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1404 - 1406
反应条件
in 2,2,4-trimethylpentane
T=-25.1 - 68.9°C; Irradiationvarious of solvent and temperature, ΔE excit; Thermodynamic dataMechanismRate constant;
参考文献
Griller; Nazran; Scaiano
Journal of the American Chemical Society, 1984 , vol. 106, # 1 p. 198 - 202