H-GLU(GLN-OH)-OH合成路线 （共 15 条）
反应条件
hydrogen; palladium in methanol; acetic acid 5 h;
参考文献
Noda, Kosaku; Igata, Keiko; Horikawa, Yoshiko; Fujii, Hisao
Agricultural and Biological Chemistry, 1980 , vol. 44, # 10 p. 2419 - 2424
反应条件
Tris buffer (pH: 8.8) T=37°C; 2 h; transamidase from Bacillus natto; Yield given;
参考文献
Morelli, Carlo F.; Calvio, Cinzia; Biagiotti, Marco; Speranza, Giovanna
FEBS Journal, 2014 , vol. 281, # 1 p. 232 - 245
反应条件
1: DCC / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) r.t., 5 h 2: Et3N / dimethylformamide; H2O / 24 h / Ambient temperature 3: 84 percent / H2 / Pd black / aq. acetic acid; methanol / 5 h View Scheme
参考文献
Sachs; Brand
Journal of the American Chemical Society, 1954 , vol. 76, p. 3601
反应条件
sodium hydroxide; Escherichia coli K-12 SH642 γ-glutamyltranspeptidase T=37°C; pH=10; 3 h;
参考文献
Suzuki, Hideyuki; Kato, Kenji; Kumagai, Hidehiko
Journal of Agricultural and Food Chemistry, 2004 , vol. 52, # 3 p. 577 - 580
反应条件
1: Et3N / dimethylformamide; H2O / 24 h / Ambient temperature 2: 84 percent / H2 / Pd black / aq. acetic acid; methanol / 5 h View Scheme
参考文献
Noda, Kosaku; Igata, Keiko; Horikawa, Yoshiko; Fujii, Hisao
Agricultural and Biological Chemistry, 1980 , vol. 44, # 10 p. 2419 - 2424
反应条件
glutaminase from Aspergillus oryzae T=30°C; 8 h; pH=8.5 (tris-HCl buffer);
参考文献
Tomita, Kenji; Yano, Toshihiro; Kitagata, Tatsuichiro; Kumagai, Hidehiko; Tochikura, Tatsurokuro
Agricultural and Biological Chemistry, 1989 , vol. 53, # 7 p. 1995 - 1996
反应条件
glutaminase from Aspergillus oryzae T=30°C; pH=8.5 (tris-HCl buffer); Yield given;
参考文献
Tomita, Kenji; Yano, Toshihiro; Kitagata, Tatsuichiro; Kumagai, Hidehiko; Tochikura, Tatsurokuro
Agricultural and Biological Chemistry, 1989 , vol. 53, # 7 p. 1995 - 1996
反应条件
1: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.03 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction 2: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.33 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction View Scheme
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 74, # 9 p. 1936 - 1939
反应条件
1: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.03 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction 2: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.33 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction View Scheme
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 74, # 9 p. 1936 - 1939
反应条件
1: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.03 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction 2: 1H-imidazole; recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase; hydroxylamine / water / 0.33 h / 30 °C / pH 7.5 / Enzymatic reaction View Scheme
参考文献
Imaoka, Masashi; Yano, Shigekazu; Okumura, Masashi; Hibi, Takao; Wakayama, Mamoru
Bioscience, Biotechnology and Biochemistry, 2010 , vol. 74, # 9 p. 1936 - 1939
