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distn. of (CH2CH)2BCl to SbF3 in vac. at -80°C, react. mixt. kept at -80°C for 35 h, at -25°C for 1 h, at 0°C for 1 h.; fractionation with -96°C, -116°C and -196°C cold traps; (CH2CH)2BF collected at -116°C, CH2CHBF2 at -196°C;

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SbF3

comproportion;