反应条件
1: [Ir2(OMe)2(1,5-cyclooctadiene)2]; 4,4'-di-tert-butyl-2,2'-dipyridyl / tetrahydrofuran / 40 h / 80 °C / |Inert atmosphere
2: dihydrogen peroxide; sodium hydroxide / methanol; tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere
3: oxygen; (R,R)-Cr(salen)Cl / 1,2-dichloro-ethane / 24 h / 85 °C / |Inert atmosphere
View Scheme
参考文献
Lee, Young Eun; Cao, Trung; Torruellas, Carilyn; Kozlowski, Marisa C.
Journal of the American Chemical Society, 2014 , vol. 136, # 19 p. 6782 - 6785