4-苯基磺酰基-苯甲酸乙酯合成路线 (共 11 条)
反应条件
pyridine; zinc; CoI2(dppe) in acetonitrile T=80°C; 10 h;
参考文献
Wong, Ying-Chieh; Jayanth, Thiruvellore Thatai; Cheng, Chien-Hong
Organic Letters, 2006 , vol. 8, # 24 p. 5613 - 5616
反应条件
1,10-phenanthroline; oxygen; anhydrous copper acetate in dimethyl sulfoxide T=100°C; 3 h; Air atmosphere;
参考文献
Yasuike, Shuji; Nishioka, Motokazu; Kakusawa, Naoki; Kurita, Jyoji
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6403 - 6406
反应条件
tetrabutyl ammonium fluoride in acetonitrile T=75°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
Yu, Xiao-Chun; Li, Bo; Yu, Bao-Hua; Xu, Qing
Chinese Chemical Letters, 2013 , vol. 24, # 7 p. 605 - 608
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
反应条件
copper(I) sulphide; iron; potassium carbonate; dimethyl sulfoxide T=90°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Wang, Huifeng; Jiang, Linlin; Chen, Tao; Li, Yarning
European Journal of Organic Chemistry, 2010 , # 12 p. 2324 - 2329
反应条件
copper(II) ferrite; potassium tert-butylate in 1,4-dioxane 24 h; RefluxInert atmosphere;
参考文献
Panda, Niranjan; Jena, Ashis Kumar; Mohapatra, Sasmita
Applied Catalysis A: General, 2012 , vol. 433-434, p. 258 - 264
反应条件
1: p-EtOC(O)C6H4Cl With palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=20°C; 0.0833333 h; Inert atmosphere; 2: In(SPh)3 With caesium carbonate in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Atobe, Shingo; Sonoda, Motohiro; Suzuki, Yuki; Shinohara, Hiroyuki; Yamamoto, Takuya; Ogawa, Akiya
Chemistry Letters, 2011 , vol. 40, # 9 p. 980 - 982
反应条件
copper(II) ferrite; potassium tert-butylate in 1,4-dioxane 24 h; RefluxInert atmosphere;
参考文献
Panda, Niranjan; Jena, Ashis Kumar; Mohapatra, Sasmita
Applied Catalysis A: General, 2012 , vol. 433-434, p. 258 - 264
反应条件
(i) aq. HCl, (ii) NaNO2, H2O, (iii) /BRN= 506523/, NaOH; Multistep reaction;
参考文献
Truce,W.E. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2872 - 2876