2-烯丙基-2-(2-丙炔基)丙二酸二乙酯合成路线 (共 29 条)
反应条件
palladium diacetate; formic acid; triphenylphosphine in 1,4-dioxane
T=70°C; 2 h; reductive elimination of enynes using other Pd-catalyst; solvent effect; Product distribution;
参考文献
Oh, Chang Ho; Jung, Hyung Hoon
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1535 - 1538
反应条件
Grubb's 2nd generation catalyst; N,N-dimethyl-formamide in toluene
0.333333 h; Inert atmosphereReflux;
参考文献
Mallagaray, Alvaro; Mohammadiannejad-Abbasabadi, Kazem; Medina, Sandra; Dominguez, Gema; Perez-Castells, Javier
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 33 p. 6665 - 6672
反应条件
piperidine; formic acid; palladium diacetate; triphenylphosphine in acetonitrile
0.0166667 h; Heating;
参考文献
Grigg, Ronald; Stevenson, Paul; Worakun, Tanachat
Tetrahedron, 1988 , vol. 44, # 15 p. 4967 - 4972
反应条件
palladium diacetate; formic acid; triphenylphosphine in 1,4-dioxane
T=70°C; 2 h; reductive elimination of enynes using other Pd-catalyst; solvent effect; Product distribution;
参考文献
Oh, Chang Ho; Jung, Hyung Hoon
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1535 - 1538
反应条件
resin supported(phosphine-(CO)3Co-Co(CO)3-phosphine) in tetrahydrofuran
T=70°C; intramolecular Pauson-Khand reaction; P=760.051 Torr; 24 h; Product distribution; Further Variations:Catalysts;
参考文献
Dahan, Adi; Portnoy, Moshe
Chemical Communications, 2002 , # 22 p. 2700 - 2701
反应条件
4 A molecular sieve; [Rh(1,5-cod)Biphemp]OTf in toluene
T=0°C; 4 h; Product distribution; Further Variations:CatalystsPressuresSolventsTemperatures;
参考文献
Schmid, Thomas M.; Consiglio, Giambattista
Chemical Communications, 2004 , # 20 p. 2318 - 2319
反应条件
Wilkinson's catalyst in acetonitrile
24 h; Heating;
参考文献
Grigg, Ronald; Stevenson, Paul; Worakun, Tanachat
Tetrahedron, 1988 , vol. 44, # 15 p. 4967 - 4972
反应条件
trifuran-2-yl-phosphane; acetic acid; trifluoroacetic acid; palladium diacetate in ethylene glycol dimethyl ether
T=80°C; P=1520.1 Torr; 24 h;
参考文献
Aggarwal, Varinder K.; Butters, Mike; Davies, Paul W.
Chemical Communications, 2003 , # 9 p. 1046 - 1047
反应条件
indium(III) chloride in toluene
T=80°C; 2 h;
参考文献
Fourmy, Kevin; Mallet-Ladeira, Sonia; Dechy-Cabaret, Odile; Gouygou, Maryse
Organometallics, 2013 , vol. 32, # 6 p. 1571 - 1574