(2-氯-6-硝基苯基)甲胺合成路线 （共 6 条）
反应条件
1: With borane-THF in DMF (N,N-dimethyl-formamide) T=0 - 20°C; 15 h; 2: With hydrogenchloride in DMF (N,N-dimethyl-formamide); water 2.5 h; Heating / reflux; 3: With sodium hydroxide in water
参考文献
Huang, Qi; Kaller, Matthew; Nguyen, Thomas; Norman, Mark H.; Rzasa, Robert; Wang, Hui-Ling; Zhong, Wenge
Patent: US2003/229068 A1, 2003 ;
Location in patent: Page 49 ;
US 20030229068 A1
反应条件
1: N-bromosuccinimide 2: dimethylformamide / 2 h / Ambient temperature 3: 1.) hydrazin-hydrate, 2.) HCl / 1.) MeOH, 1 h, reflux, 2.) H2O, MeOH View Scheme
参考文献
Stalder
Helvetica Chimica Acta, 1986 , vol. 69, # 8 p. 1887 - 1897
反应条件
1: dimethylformamide / 2 h / Ambient temperature 2: 1.) hydrazin-hydrate, 2.) HCl / 1.) MeOH, 1 h, reflux, 2.) H2O, MeOH View Scheme
参考文献
Stalder
Helvetica Chimica Acta, 1986 , vol. 69, # 8 p. 1887 - 1897
反应条件
hydrogenchloride; hydrazine hydrate 1.) MeOH, 1 h, reflux, 2.) H2O, MeOH; Yield given. Multistep reaction;
参考文献
Stalder
Helvetica Chimica Acta, 1986 , vol. 69, # 8 p. 1887 - 1897
反应条件
und Erhitzen des Reaktionsprodukts mit wss.HCl;
参考文献
Southwick; Cremer
Journal of Organic Chemistry, 1959 , vol. 24, p. 753
反应条件
nickel in ethanol Ambient temperature; Yield given;
参考文献
Stalder
Helvetica Chimica Acta, 1986 , vol. 69, # 8 p. 1887 - 1897
