2-甲氧基-4-硝基苯甲腈合成路线 （共 21 条）
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2226,2235
反应条件
T=25°C; other dinitrobenzonitrile, other solvent; Rate constantMechanism;
参考文献
Journal of Chemical Research, Miniprint, , # 6 p. 1371 - 1382
反应条件
lithium chloride T=160°C;
参考文献
YALE UNIVERSITY
Patent: WO2007/38387 A2, 2007 ;
Location in patent: Page/Page column 24; 25 ;
参考文献
Clinton et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3674,3678
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 1 h;
参考文献
Synthesis, , # 19 p. 3316 - 3340
反应条件
sulfuric acid anschliessendes Erwaermen mit wss. NaNO2;
参考文献
Clinton et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 592,595
反应条件
1: aqueous H2SO4 / anschliessendes Erwaermen mit wss. NaNO2 2: iron-powder; aq.-ethanolic HCl View Scheme
参考文献
Clinton et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 592,595
反应条件
1: 100 percent / LiCl / 160 °C
2: 70 percent / SnCl2*2H2O; aq. HCl
View Scheme
参考文献
Ruiz-Caro, Juliana; Basavapathruni, Aravind; Kim, Joseph T.; Bailey, Christopher M.; Wang, Ligong; Anderson, Karen S.; Hamilton, Andrew D.; Jorgensen, William L.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 3 p. 668 - 671
反应条件
1: acetic acid; H2SO4; aqueous HBr
2: Na2CO3; NaI; ethanol
3: aq.-ethanolic Na2CO3
4: SOCl2; pyridine; benzene / anschliessendes Behandeln mit 2-Dimethylamino-aethanol
5: palladium/charcoal; aq.-ethanolic HCl / Hydrogenation
6: zinc-powder; acetic acid; benzene
View Scheme
参考文献
Clinton et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3674,3678
反应条件
hydrogenchloride; water
1.) ether, 12 h, RT, 2.) ether, 30 min, 60 deg C; Yield given. Multistep reaction;
参考文献
Imakura; Okimoto; Konishi; Hisazumi; Yamazaki; Kobayashi; Yamashita
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 7 p. 1691 - 1696
