反应条件
in neat (no solvent) byproducts: Br2, FNO; Irradiation (UV/VIS); irradiated for 12 h with λmax = 420 nm; condensed into a cylinder held at -196°C, vac. transferred into another cylinder, condensed several times (trap-to-trap); obtained with apurity of ca 98percent;
参考文献
Lu, Norman; Thrasher, Joseph S.; Von Ahsen, Stefan; Willner, Helge; Hnyk, Drahomir; Oberhammer, Heinz
Inorganic Chemistry, 2006 , vol. 45, # 4 p. 1783 - 1788