3-苯基-1,3-噻唑烷-2,4-二酮合成路线 (共 72 条)
反应条件
1: various solvent(s) / Heating
2: ethanol / 6 h / Heating
3: conc. HCl / various solvent(s) / 8 h / Heating
View Scheme
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
1: ethanol / 6 h / Heating
2: conc. HCl / various solvent(s) / 8 h / Heating
View Scheme
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
1: ethanol / 6 h / Heating
2: conc. HCl / various solvent(s) / 8 h / Heating
View Scheme
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
1: NaOAc / acetic acid / Heating
2: aq. HCl / Heating
View Scheme
参考文献
Vladzimirskaya,E.V.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 2774 - 2776,2796 - 2798
反应条件
1: NaOAc / ethanol / Heating
2: aq. H2SO4 / Heating
View Scheme
参考文献
Condon,F.E.; Trivedi,J.P.
Journal of the Indian Chemical Society, 1971 , vol. 48, p. 597 - 598
反应条件
1: ethanol
2: aq. HCl / dioxane / 1 h / Heating
View Scheme
参考文献
Svetkin,Y.V. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 751 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 903 - 905
反应条件
1: ethanol / 8 h / Reflux
2: sodium acetate / acetic acid / 24 h / Reflux
3: hydrogenchloride / ethanol
View Scheme
参考文献
Ragab, Fatma Abd El-Fattah; Hassan, Ghaneya Sayed; Abu Yossef, Hanan Al-Sayed; Yahya, Tawfeek Ahmed Ali; Abd El-Latif, Hekma A.
Arzneimittel-Forschung/Drug Research, 2010 , vol. 60, # 4 p. 171 - 176
反应条件
hydrogenchloride
7 h; Heating;
参考文献
Potts,K.T. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 1633 - 1638
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781