4,4'-二甲氧基二苯安合成路线 （共 60 条）
反应条件
sodium t-butanolate; 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran T=100°C; 3 h;
参考文献
7TM PHARMA A/S
Patent: WO2007/62797 A1, 2007 ;
Location in patent: Page/Page column 26 ;
WO 2007/062797 A1
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate in toluene T=90°C; Buchwald-Hartwig coupling; 24 h; Inert atmosphere;
参考文献
Li, Yilin; Scudiero, Louis; Ren, Tianhui; Dong, Wen-Ji
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 231, # 1 p. 51 - 59
反应条件
C21H16CuN2O2; potassium carbonate in water T=28°C; Chan-Lam Coupling; 21 h;
参考文献
Gogoi, Ankur; Sarmah, Gayatri; Dewan, Anindita; Bora, Utpal
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 31 - 35
反应条件
Pd-PEPPSI-IPent; caesium carbonate in ethylene glycol dimethyl ether T=80°C; 24 h; Inert atmosphere;
参考文献
Hoi, Ka Hou; Calimsiz, Selcuk; Froese, Robert D. J.; Hopkinson, Alan C.; Organ, Michael G.
Chemistry - A European Journal, 2012 , vol. 18, # 1 p. 145 - 151
反应条件
potassium tert-butylate; copper(l) iodide; tributylphosphine in toluene T=135°C; 10.5 h; high pressure;
参考文献
Chemical Communications, , # 19 p. 2460 - 2461
反应条件
potassium tert-butylate; copper(l) iodide; tributylphosphine in toluene T=135°C; 10.5 h; high pressure;
参考文献
Chemical Communications, , # 19 p. 2460 - 2461
反应条件
Pd[P(o-tol)3]2; CyPF-t-Bu; ammonia; sodium t-butanolate in 1,4-dioxane T=100°C; 15 h; Inert atmosphere;
参考文献
Vo, Giang D.; Hartwig, John F.
Journal of the American Chemical Society, 2009 , vol. 131, # 31 p. 11049 - 11061
反应条件
ammonia; copper (II) acetate monohydrate; benzoic acid in water; propionic acid ethyl ester T=80°C; 24 h;
参考文献
Zhou, Changfeng; Chen, Fan; Yang, Dongpeng; Jia, Xiaofei; Zhang, Lixue; Cheng, Jiang
Chemistry Letters, 2009 , vol. 38, # 7 p. 708 - 709
反应条件
lithium perchlorate; potassium carbonate; platinum; mercury in acetonitrile T=0°C; 3 h; Electrochemical reaction;
参考文献
Electrochemistry Communications, , vol. 12, # 7 p. 973 - 976
反应条件
1: Condensation; Ullmann reaction; 2: With potassium hydroxide in ethanol Hydrolysis; Further stages.;
参考文献
Selby, Trent D.; Stickley, Kurt R.; Blackstock, Silas C.
Organic Letters, 2000 , vol. 2, # 2 p. 171 - 174
