双[4-(二甲氨基)苯基]甲烷合成路线 (共 236 条)
反应条件
potassium hydroxide; hydrazine hydrate in diethylene glycol T=130 - 140°C; 1.5 h;
参考文献
Streitwieser, Andrew Jr.; Vorpagel, Erich R.; Chen, Chia-Chung
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 6970 - 6975
反应条件
FeCl3·6H2O; triethylamine in toluene T=85°C; 2 h;
参考文献
Ling, Xuege; Xiong, Yan; Huang, Ruofeng; Zhang, Xiaohui; Zhang, Shuting; Chen, Changguo
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5218 - 5226
反应条件
acetic acid; β-naphthol in ethanol T=20°C; Mannich type Friedel-Crafts reaction; 12 h;
参考文献
Kumar, Atul; Kumar, Mukesh; Gupta, Maneesh Kumar
Tetrahedron Letters, 2009 , vol. 50, # 50 p. 7024 - 7027
反应条件
tetrahydrofuran; palladium diacetate in acetic acid T=50°C; 19 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 107, p. 6417
反应条件
1: With antimony(V) pentachloride in dichloromethane T=20°C; 24 h; Inert atmosphere; 2: in dichloromethane T=20°C; 1 h; Inert atmosphereRefluxAlkaline conditions; Concentration;
参考文献
Arkivoc, , vol. 2013, # 3 p. 36 - 48
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform T=25°C; 10 h; TimeTemperatureReagent/catalyst;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide; isopropyl alcohol T=80°C; 8 h;
参考文献
Barbero, Margherita; Bazzi, Stefano; Cadamuro, Silvano; Dughera, Stefano; Ghigo, Giovanni
European Journal of Organic Chemistry, 2009 , # 25 p. 4346 - 4351
反应条件
ytterbium 20 h; Ambient temperature;
参考文献
Chemistry Letters, , # 3 p. 611 - 614
反应条件
aluminum oxide in dichloromethane T=20°C; 20 h;
参考文献
Lai, Yu-Ying; Lin, Nai-Ti; Liu, Yi-Hung; Wang, Yu; Luh, Tien-Yau
Tetrahedron, 2007 , vol. 63, # 26 p. 6051 - 6055
反应条件
palladium diacetate in acetic acid T=50°C; 19 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 107, p. 6417