1,3-二氯-5-甲氧基-2-硝基苯合成路线 (共 8 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C; 1 h;
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
sulfuric acid; nitric acid in dichloromethane T=20°C; 18 h; Title compound not separated from byproducts;
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C; Methylation; 1 h;
参考文献
Waterhouse, Ian
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 11 p. 1075 - 1083
反应条件
1: diluted sulfuric acid; sodium nitrate 2: potassium carbonate; xylene View Scheme
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
sodium dithionite in ethanol; water 14 h; Heating;
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
tin in hydrogenchloride Reduction; 1 h; Heating;
参考文献
Waterhouse, Ian
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 11 p. 1075 - 1083
参考文献
Hodgson; Wignall
Journal of the Chemical Society, 1928 , p. 331
反应条件
tin in hydrogenchloride
Reduction; 1 h; Heating;
参考文献
Waterhouse, Ian
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 11 p. 1075 - 1083