甲基 2-乙酰氨基-2-脱氧-3-O-己糖吡喃糖苷吡喃己糖苷合成路线 （共 10 条）
反应条件
sodium methylate in methanol
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2068
反应条件
sodium phosphate buffer pH 6.5; β-D-galactopyranose in N,N-dimethyl-formamide T=37°C; 1680 h;
参考文献
Carbohydrate research, , vol. 188, p. 9 - 17
反应条件
1: 50percent aq. CH3COOH / 100 °C 2: NaOCH3 / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2068
反应条件
1: toluene sulfonic acid monohydrate / acetonitrile; dimethylformamide / 3 h / 70 °C 2: Hg(CN)2 / benzene; nitromethane 3: 50percent aq. CH3COOH / 100 °C 4: NaOCH3 / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2068
反应条件
1: Hg(CN)2 / benzene; nitromethane 2: 50percent aq. CH3COOH / 100 °C 3: NaOCH3 / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2068
反应条件
1: 86 percent / TsOH*H2O / acetonitrile / 16 h / 20 °C 2: 1) MS4A, 2) nitrosyl tetrafluoroborate / 1) CH2Cl2, 20 deg C, 45 min, 2) 20 deg C, 1 h 3: 81 percent / trifluoroacetic acid / CHCl3; H2O / 0.67 h 4: hydrazine hydrate / aq. ethanol / 10 h / Heating 5: methanol; H2O / 17 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 226, # 2 p. 331 - 336
反应条件
1: 1) MS4A, 2) nitrosyl tetrafluoroborate / 1) CH2Cl2, 20 deg C, 45 min, 2) 20 deg C, 1 h 2: 81 percent / trifluoroacetic acid / CHCl3; H2O / 0.67 h 3: hydrazine hydrate / aq. ethanol / 10 h / Heating 4: methanol; H2O / 17 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 226, # 2 p. 331 - 336
反应条件
1: hydrazine hydrate / aq. ethanol / 10 h / Heating 2: methanol; H2O / 17 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 226, # 2 p. 331 - 336
反应条件
1: 81 percent / trifluoroacetic acid / CHCl3; H2O / 0.67 h 2: hydrazine hydrate / aq. ethanol / 10 h / Heating 3: methanol; H2O / 17 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 226, # 2 p. 331 - 336
反应条件
in methanol; water T=20°C; 17 h; Yield given;
参考文献
Carbohydrate Research, , vol. 226, # 2 p. 331 - 336
