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结构式
乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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2-苯基吡啶
合成路线
（共 355 条）
188527-50-6
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
tri-ruthenium(0)dodecacarbonyl; carbon monoxide in toluene T=160°C; decarbonylative cleavage; P=3800 Torr; 20 h;
参考文献
Chatani, Naoto; Ie, Yutaka; Kakiuchi, Fumitoshi; Murai, Shinji
Journal of the American Chemical Society, 1999 , vol. 121, # 37 p. 8645 - 8646
109-09-1
2-氯吡啶
+
100-58-3
溴化苯基镁
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
[1,3-bis(2,6-diisopropylphenyl)-imidazolium][Ni(PPh3)Cl3] in tetrahydrofuran T=30°C; Kumada Cross-Coupling; 5 h; Schlenk techniqueInert atmosphere;
参考文献
Xu, Yan-Chao; Zhang, Jie; Sun, Hong-Mei; Shen, Qi; Zhang, Yong
Dalton Transactions, 2013 , vol. 42, # 23 p. 8437 - 8445
108-86-1
溴代苯
+
25108-36-5
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
pyridine; copper(I) oxide; triphenylphosphine; PdI2 in 1-methyl-pyrrolidin-2-one T=50 - 190°C; 6 h; Microwave irradiationInert atmosphere; Reagent/catalystConcentrationTime;
参考文献
Haley, Christopher K.; Gilmore, Christopher D.; Stoltz, Brian M.
Tetrahedron, 2013 , vol. 69, # 27-28 p. 5732 - 5736
109-04-6
邻溴吡啶
+
143-66-8
四苯硼钠
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
palladium diacetate; sodium carbonate in various solvent(s) Suzuki reaction; 0.2 h; microwave irradiation;
参考文献
Villemin, Didier; Gomez-Escalonilla, Maria Jose; Saint-Clair, Jean-Francois
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 635 - 637
109-04-6
邻溴吡啶
+
2633-57-0
(三-2-丙烯-1-基硅烷基)-苯
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 23 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
386253-27-6
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran T=25°C;
参考文献
Charette; Grenon; Lemire; Pourashraf; Martel
Journal of the American Chemical Society, 2001 , vol. 123, # 47 p. 11829 - 11830
5029-67-4
2-碘吡啶
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1: Bromure de phenyl magnesium With indium(III) chloride in tetrahydrofuran T=25°C; 2: 2-iodo-pyridine With tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane in tetrahydrofuran; water 5 h; Heating; Further stages.;
参考文献
Takami, Kazuaki; Yorimitsu, Hideki; Shinokubo, Hiroshi; Matsubara, Seijiro; Oshima, Koichiro
Organic Letters, 2001 , vol. 3, # 13 p. 1997 - 1998
372-48-5
2-氟吡啶
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) in diethyl ether T=20°C; 2 h;
参考文献
Yoshikai, Naohiko; Mashima, Hiroko; Nakamura, Eiichi
Journal of the American Chemical Society, 2005 , vol. 127, # 51 p. 17978 - 17979
109-04-6
邻溴吡啶
+
100-58-3
溴化苯基镁
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1: phenyl-magnesium bromide With titanium tetraethoxide in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: 2-bromo-pyridine With tributylphosphine; cobalt(II) chloride in tetrahydrofuran T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Zeng, Jing; Liu, Kun Ming; Duan, Xin Fang
Organic Letters, 2013 , vol. 15, # 20 p. 5342 - 5345
100-70-9
+
100-59-4
苯基氯化镁
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
lithium tert-butylate; [NiCl2(PMe3)2] in tetrahydrofuran T=25°C; 24 h;
参考文献
Miller, Joseph A.
Tetrahedron Letters, 2001 , vol. 42, # 40 p. 6991 - 6993
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