5-甲基-3-苯基异噁唑合成路线 （共 67 条）
反应条件
1: in dichloromethane T=30°C; 2 h; 2: With triethylamine in dichloromethane T=40°C; 24 h;
参考文献
Kurkowska, Joanna; Zadrozna, Irmina
Journal of Chemical Research, Miniprint, 2003 , # 5 p. 541 - 554
反应条件
triethylamine in diethyl ether 20 h;
参考文献
Kobayashi, Tomoshige; Nitta, Makoto
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 152 - 157
反应条件
copper in quinoline Heating;
参考文献
Cahiez, Gerard; Moyeux, Alban; Gager, Olivier; Poizat, Mael
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 790 - 796
反应条件
hydroxylamine hydrochloride; sodium ethanolate in ethanol
参考文献
Kashima, Choji; Shirai, Shun-ichi; Yoshiwara, Nobutoshi; Omote, Yoshimori
Journal of the Chemical Society, Chemical Communications, 1980 , # 17 p. 826 - 827
反应条件
sodium hydroxide in water 7 h; Heating;
参考文献
Fitton, Alan O.; Patel, Rajeshkumar N.; Millar, Ross W.
Journal of Chemical Research, Miniprint, 1986 , # 4 p. 1101 - 1127
反应条件
hydroxylamine hydrochloride in methanol 8 h; Heating;
参考文献
Rodriguez, Antoniom.; Juan, Alberto; Gomez, M.Victoria; Moreno, Andres; De La Hoz, Antonio
Synthesis (Germany), 2012 , vol. 44, # 16 p. 2527 - 2530
反应条件
1: With triethylamine in chloroform T=20°C; 12 h; 2: With dihydrogen peroxide in chloroform T=20°C; 0.333333 h; Title compound not separated from byproducts;
参考文献
Sheng, Shou-Ri; Liu, Xiao-Ling; Xu, Qu; Song, Cai-Sheng
Synthesis, 2003 , # 18 p. 2763 - 2764
反应条件
1: propargyl bromide With iodine; magnesium; mercury dichloride in tetrahydrofuran; toluene T=20°C; 2 h; 2: BNO in tetrahydrofuran; toluene 5 h;
参考文献
Sampath Kumar; Singh, Parvinder Pal; Shafi, Syed; Reddy, Pitta Bhaskar; Shravankumar, Kankala; Reddy, Doma Mahender
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 887 - 890
反应条件
1.1: BuLi / tetrahydrofuran; hexane / -40 °C 1.2: tetrahydrofuran; hexane / -40 - 20 °C 2.1: conc. H2SO4 / 80 °C View Scheme
参考文献
Dileep Kumar; Ho, ManKit M.; Leung, Jennifer M.; Toyokuni, Tatsushi
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 10 p. 1146 - 1151
反应条件
in diethyl ether 20 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Rastelli, Augusto; Bagatti, Marisa; Gandolfi, Remo
Journal of the American Chemical Society, 1995 , vol. 117, # 17 p. 4965 - 4975
