sodium hydride in N,N-dimethyl-formamide T=25°C; 0.666667 h;
参考文献
Novikov, V. L.; Balaneva, N. N.; Moiseenkov, A. M.; Elyakov, G. B.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 8.2 p. 1901 - 1910,1485 - 1494
1.1: AlCl3, aluminium chloride; sodium chloride / neat (no solvent) / 0.03 h / 180 °C 2.1: tin(ll) chloride; hydrogenchloride / water / 5 h / 140 °C 3.1: potassium hydride / N,N-dimethyl-formamide / -35 - 40 °C / |Inert atmosphere 3.2: |Inert atmosphere View Scheme
参考文献
Guerrero-Vasquez, Guillermo A.; Andrade, Carlos Kleber Z.; Molinillo, Jose M. G.; MacIas, Francisco A.
European Journal of Organic Chemistry, 2013 , # 27 p. 6175 - 6180
1.1: tin(ll) chloride; hydrogenchloride / water / 5 h / 140 °C 2.1: potassium hydride / N,N-dimethyl-formamide / -35 - 40 °C / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Guerrero-Vasquez, Guillermo A.; Andrade, Carlos Kleber Z.; Molinillo, Jose M. G.; MacIas, Francisco A.
European Journal of Organic Chemistry, 2013 , # 27 p. 6175 - 6180
