反应条件
sodium tetrahydroborate; oxygen; methylene blue; Hg(NO3)2
1.) tetrachloromethane-methanol, irradiation, 16 h, 2.) dichloromethane, room temperature, 24 h, 3.) water, tetrahydrofuran, 0 deg C, 65 min; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Bascetta, Emanuele; Gunstone, Frank D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2207 - 2216