5-氯-2-甲基苯并噻唑合成路线 （共 39 条）
参考文献
Russian Journal of Organic Chemistry, , vol. 40, # 2 p. 228 - 231
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 2-methyl-5-chloro-benzothiazole With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 12 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: With palladium diacetate; xantphos in N-dodecane; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; 1 h; Inert atmosphereGlovebox; 2: With cesium hydroxide monohydrate in N-dodecane; water; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; Inert atmosphereGlovebox;
参考文献
Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259,12
Title/Abstract Full Text Show Details
Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259
参考文献
Mistr,A. et al.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 150 - 163
反应条件
Herrmann's palladacycle; C29H45Pt; potassium carbonate in water; N,N-dimethyl-formamide T=115°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Yu, Chao-Wu; Chen, Grace S.; Huang, Chen-Wei; Chern, Ji-Wang
Organic Letters, 2012 , vol. 14, # 14 p. 3688 - 3691
反应条件
sodium hydroxide in ethylene glycol 2.5 h; Heating;
参考文献
Hodson, Stephen J.; Bishop, Michael J.; Speake, Jason D.; Navas III, Frank; Garrison, Deanna T.; Bigham, Eric C.; Saussy Jr., David L.; Liacos, James A.; Irving, Paul E.; Jeffrey Gobel; Sherman, Bryan W.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 11 p. 2229 - 2239
反应条件
dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate in 1,4-dioxane T=60°C; 24 h; Inert atmosphere;
参考文献
Cheung, Chi Wai; Surry, David S.; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 14 p. 3734 - 3737
参考文献
Orlova; Kolchina; Shakirov; Gerasimova; Shelkovnikov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 2 p. 228 - 231
反应条件
1: in acetonitrile 5 h; Inert atmosphereMicrowave irradiation; 2: With hydrogenchloride
参考文献
Yue, Xiling; Yanez, Ciceron O.; Yao, Sheng; Belfield, Kevin D.
Journal of the American Chemical Society, 2013 , vol. 135, # 6 p. 2112 - 2115
参考文献
Russian Journal of Organic Chemistry, , vol. 40, # 2 p. 228 - 231
