3-(1,3-二噻烷-2-基)-2,4-戊二酮合成路线 （共 7 条）
反应条件
magnesium in methanol T=5°C; 24 h;
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
1: 74 percent / K2CO3 / dimethylformamide / 7 h 2: 92 percent / Mg / methanol / 24 h / 5 °C View Scheme
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
in nitromethane; dichloromethane 2 h; -70 deg C to r.t.;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 12 p. 4857 - 4868
反应条件
in ethanol 3 h; Heating;
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
hydroxylamine hydrochloride in ethanol 2 h; Heating;
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
1: 99 percent / NH2OH*HCl / ethanol / 2 h / Heating 2: 78 percent / NBS / H2O; acetonitrile / 0.17 h / -5 - 30 °C View Scheme
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
anhydrous iron chloride; ammonium hydroxide in N,N-dimethyl-formamide
T=60°C;
参考文献
Wang, Yeming; Bi, Xihe; Li, Wei-Qi; Li, Dehua; Zhang, Qian; Liu, Qun; Ondon, Brim Stevy
Organic Letters, 2011 , vol. 13, # 7 p. 1722 - 1725
