DL-1,1'-聚萘二酸合成路线 (共 10 条)
反应条件
zeolite HSZ-360 in neat (no solvent) T=60°C; 12 h;
参考文献
Ballini, Roberto; Bosica, Giovanna; Carloni, Silvia; Ciaralli, Lara; Maggi, Raimondo; Sartori, Giovanni
Tetrahedron Letters, 1998 , vol. 39, # 33 p. 6049 - 6052
反应条件
aluminium trichloride in nitrobenzene T=25°C; 8 h;
参考文献
Periasamy, Mariappan; Nagaraju, Miriyala; Kishorebabu, Neela
Synthesis, 2007 , # 24 p. 3821 - 3826
反应条件
4-(N,N-dimethlyamino)pyridine in isopropyl alcohol T=20°C;
参考文献
Schafer, Wes A.; Hobbs, Steve; Rehm, Jason; Rakestraw, David A.; Orella, Charles; McLaughlin, Mark; Ge, Zhihong; Welch, Christopher J.
Organic Process Research and Development, 2007 , vol. 11, # 5 p. 870 - 876
反应条件
phosphoric acid; trifluoroacetic anhydride in water T=50°C; 0.25 h;
参考文献
Costantino, Andrea R.; Ocampo, Romina A.; Schneider, Maria G. Montiel; Fernandez, Gustavo; Koll, Liliana C.; Mandolesi, Sandra D.
Synthetic Communications, 2013 , vol. 43, # 23 p. 3192 - 3202
反应条件
1: FeCl3·6H2O 2: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal Ali; Mahajan, Neha; Chaubey, Asha; Taneja, Subhash Chandra
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 101, p. 35 - 39
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Kazlauskas, Romas J.
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4953 - 4959
反应条件
ph=5.5; enzymatic hydrolysis using fungi Absidia glauca or Rhizopus arrhizus;
参考文献
Wu, Shih-Hsiung; Zhang, Li-Qing; Chen, Ching-Shih; Girdaukas, Gary; Sih, C. J.
Tetrahedron Letters, 1985 , vol. 26, # 36 p. 4323 - 4326
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Kazlauskas, Romas J.
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4953 - 4959
反应条件
ph=5.5; enzymatic hydrolysis using fungi Absidia glauca or Rhizopus arrhizus;
参考文献
Wu, Shih-Hsiung; Zhang, Li-Qing; Chen, Ching-Shih; Girdaukas, Gary; Sih, C. J.
Tetrahedron Letters, 1985 , vol. 26, # 36 p. 4323 - 4326
反应条件
pH=5.5; enzymatic hydrolysis using fungi Absidia glauca or Rhizopus arrhizus; Product distributionRate constant;
参考文献
Wu, Shih-Hsiung; Zhang, Li-Qing; Chen, Ching-Shih; Girdaukas, Gary; Sih, C. J.
Tetrahedron Letters, 1985 , vol. 26, # 36 p. 4323 - 4326