反应条件
HCl in hydrogenchloride Electrolysis; soln. of RuCl3 in 2n HCl is electrolysed as catholyte; subsequent concn. of the red soln. in HCl-stream under exclusion of air first at the b.p., later at 80-100°C to dryness;; drying over concd. H2SO4 in vacuum leads to a product free from Ru(IV);;
参考文献
Grube, G.; Fromm, G.
Zeitschrift fuer Elektrochemie, 1940 , vol. 46, p. 661 - 667
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Grube, G.; Nann, H.
Zeitschrift fuer Elektrochemie, 1939 , vol. 45, p. 871 - 874
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Gmelin Handbook: Ru: SVol., 88, page 283 - 285
