5-乙酰-1,2-二氢苊烯合成路线 (共 26 条)
反应条件
aluminium trichloride in 1,2-dichloro-ethane 3 h; Ambient temperature;
参考文献
Sugihara, Yoshiaki; Takeda, Hitoshi; Nakayama, Juzo
European Journal of Organic Chemistry, 1999 , # 3 p. 597 - 605
反应条件
1: acetyl chloride With AlCl3, aluminium chloride in dichloromethane Friedel Crafts acylation; 0.25 h; Cooling with ice; 2: 1,2-dihydroacenaphthylene in dichloromethane T=20°C; Friedel Crafts acylation; Cooling with ice;
参考文献
Xu, Chao; Luo, Wen-Feng; Li, Li-Jun; Yao, Shun; Song, Hang
Asian Journal of Chemistry, 2010 , vol. 22, # 5 p. 3923 - 3928
反应条件
boron trifluoride in dichloromethane T=0 - 10°C; 1 h; Yields of byproduct given;
参考文献
Hyatt, John A.; Raynolds, Peter W.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 384 - 385
反应条件
[2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl acetamide T=70°C; Dimerization; dehalogenation; 3 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 35, # 6 p. 913 - 915
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1272,1278
Journal of the American Chemical Society, , vol. 62, p. 49,51
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1740,1742
Journal of the American Chemical Society, , vol. 61, p. 1272,1278
Journal of the American Chemical Society, , vol. 62, p. 49,51
反应条件
iodine; hypophosphorous acid in acetic acid 24 h; Heating;
参考文献
Tetrahedron, , vol. 58, # 22 p. 4411 - 4415
反应条件
1: AlCl3 / CH2Cl2 2: Pd-C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1371 - 1378
反应条件
palladium on activated charcoal
参考文献
Bulletin de la Societe Chimique de France, , p. 1371 - 1378
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 244, p. 1220,1222