methanol in nitromethane byproducts: CH3Cl, HCl; addn. of methanol in nitromethane to suspn. of (Cl3PNPCl3)PCl6 in nitromethane (molar ratio 2:1) dropwise during 1 h at ambient temp.; various product ratio for various conditions; not isolated; (31)P-NMR spectroscopic monitoring;
参考文献
Phosphorus, Sulfur, and Silicon and the Related Elements, , vol. 63, p. 19 - 32