780-800°C in vac.; Two-fold vacuum sublimation with prior distilling off SiCl4.;
参考文献
Inorganic Materials (Transl. of Neorg. Mater.), , vol. 27, p. 735 - 736
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, , vol. 27, p. 875 - 876
→
反应条件
Cl2/Ar mixt. flowing over In2O3 (const. temp. in range 500-700°C,gas flow rate 2ml/min, complete satn. of carrier gas by vapours of gase ous products, duration 3 h); monitoring by gravimetric and chem. anal.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 24, p. 1446 - 1448
Zhurnal Neorganicheskoi Khimii, , vol. 24, p. 2605 - 2608
