反应条件
in dichloromethane
byproducts: Me3SiCl; N2-atmosphere; dropwise addn. of mixt. of 1 equiv. SCl2 and 1 equiv. S2Cl2 to 1 equiv. Si-compd. at -78°C, slow warming to room temp., stirring for 12 h; filtration, evapn., sublimation (room temp., < 10 Pa), recrystn. (Et2O);
参考文献
Maaninen, Arto; Siivari, Jari; Suontamo, Reijo J.; Konu, Jari; Laitinen, Risto S.; Chivers, Tristram
Inorganic Chemistry, 1997 , vol. 36, # 10 p. 2170 - 2177
