1-甲基-6-氧代-1,6-二氢吡啶-3-硼酸频那醇酯合成路线 (共 4 条)
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in dimethyl sulfoxide T=80°C; 0.5 h;
参考文献
EP2168965 A1, ;
Page/Page column 33 ;
EP 2168965 A1
反应条件
1: With triethylamine in dichloromethane T=20°C; 1 h; 2: With sodium hydroxide in 1,4-dioxane T=70°C; 1 h;
参考文献
WO2013/185284 A1, ;
Page/Page column 148 ;
反应条件
potassium carbonate in acetonitrile T=50°C; 16 h; Sealed vial;
参考文献
WO2012/125893 A1, ;
Page/Page column 212-213 ;
WO 2012/125893 A1
参考文献
WO2008/141119 A2, ;
Page/Page column 96-97 ;
WO 2008/141119 A2