反应条件
in diethyl ether; water (under Ar, Schlenk); NaBH4 in water at 0°C deoxygenated by bubbling Ar for 30 min, soln. of (CH3(CH2)3)2SnCl2 in Et2O slowly added over 45 min, stirred for 15 min; sepd., washed with water, dried over MgSO4, concd. under vac.;
参考文献
Hernan, Alejandro G.; Horton, Peter N.; Hursthouse, Michael B.; Kilburn, Jeremy D.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 8 p. 1466 - 1475
