2-氨基-2-甲基丙烷盐酸盐合成路线 （共 44 条）
反应条件
N,N-dichloro-2-methyl-2-propanamine in tetrachloromethane
T=20°C; 1 h; Irradiationother alcohol; MechanismProduct distribution;
参考文献
Ogata, Yoshiro; Kimura, Makoto
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 947 - 950
反应条件
in diethyl ether
byproducts: HCl; in presence of a trap for HCl;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
in benzene
very slow addn. of t-butylamine in benzene to TiCl4 in benzene cooled to ice-water temp., stirred for 18 h (ice-bath removed); (CH3)3NH3Cl filtered off, removal of solvent, extn. (warm petroleum ether), filtered, volume reduced, dried in vac.; elem. anal.;
参考文献
Nielson, Alastair J.
Inorganica Chimica Acta, 1988 , vol. 154, p. 177 - 182
反应条件
N,N-dichloro-2-methyl-2-propanamine in tetrachloromethane
T=20°C; 1 h; Irradiation; Product distribution;
参考文献
Ogata, Yoshiro; Kimura, Makoto
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 947 - 950
反应条件
N,N-dichloro-2-methyl-2-propanamine in tetrachloromethane
T=20°C; 1 h; Irradiation; Product distribution;
参考文献
Ogata, Yoshiro; Kimura, Makoto
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 947 - 950
反应条件
titanium(IV) isopropylate in tetrahydrofuran; diethyl ether
Grignard reaction; Cyclization; 240 h; Heating;
参考文献
De Meijere, Armin; Chaplinski, Vladimir; Gerson, Fabian; Merstetter, Pascal; Haselbach, Edwin
Journal of Organic Chemistry, 1999 , vol. 64, # 19 p. 6951 - 6959
反应条件
hydrogenchloride; triethyl phosphite in benzene
1.) room temp., overnight, 2.) room temp., overnight; Yield given;
参考文献
Koziara, Anna; Osowska-Pacewicka, Krystyna; Zawadzki, Stefan; Zwierzak, Andrzej
Synthesis, 1987 , # 5 p. 487 - 489
参考文献
Brander
Recueil des Travaux Chimiques des Pays-Bas, 1918 , vol. 37, p. 83
反应条件
in toluene
24 h; Heating;
参考文献
Murugavel, Ramaswamy; Pothiraja, Ramasamy
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 968 - 974
反应条件
in pentane
dropwise addn. of amine in pentane to borane in pentane at -0°C, stirred for 2 h at room temp.; filtered, distn. (44°C/8 Torr); elem. anal.;
参考文献
Kuepper, Stefan; Paetzold, Peter; Boese, Roland
Chemische Berichte, 1993 , vol. 126, # 8 p. 1787 - 1790
