5-甲基-2(3H)-呋喃酮合成路线 (共 25 条)
反应条件
bis(benzonitrile)palladium(II) dichloride; triethylamine in tetrahydrofuran T=60°C; 6 h; Inert atmosphere;
参考文献
Heterocycles, , vol. 86, # 2 p. 947 - 954
反应条件
iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene 2.) benzene; Multistep reaction;
参考文献
Agricultural and Biological Chemistry, , vol. 50, # 3 p. 625 - 631
参考文献
Lang, Robert W.; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1980 , vol. 63, # 5 p. 1204 - 1214
反应条件
1: Jones reagent 2: HgO / benzene / 0.75 h / Heating; further reagent and solvents; solvent effect View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 582 - 587
反应条件
1: 83 percent / I2 / CCl4 / 24 h / Heating 2: 79 percent / DBU / benzene / 3 h / 70 - 80 °C View Scheme
参考文献
Liebigs Annalen der Chemie, , # 1 p. 15 - 30
反应条件
iodine in cyclohexane T=25 - 150°C; ΔG0, ΔH0, ΔS0; Thermodynamic dataEquilibrium constant;
参考文献
Tetrahedron, , vol. 50, # 6 p. 1885 - 1888
反应条件
mercury(II) oxide 4 h; Heating;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 991 - 992
反应条件
mercury(II) oxide 1 h; Heatingvar. time; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 991 - 992
反应条件
mercury(II) oxide 4 h; Heating;
参考文献
Yamamoto, Makoto; Yoshitake, Makoto; Yamada, Kazutoshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 991 - 992
反应条件
hydrogen; Ru(OCOCH3)2((R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl) in dichloromethane T=50°C; P=76000 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fehr, Matthias J.; Consiglio, Giambattista; Scalone, Michelangelo; Schmid, Rudolf
Journal of Organic Chemistry, 1999 , vol. 64, # 16 p. 5768 - 5776