3,6-双(5-溴-2-噻吩基)-2,5-双(2-乙基己基)-2,5-二氢吡咯并[3,4-c]吡咯-1,4-二酮合成路线 （共 3 条）
反应条件
N-bromosuccinmide in chloroform T=0 - 20°C;
参考文献
Woo, Claire H.; Beaujuge, Pierre M.; Holcombe, Thomas W.; Lee, Olivia P.; Frechet, Jean M. J.
Journal of the American Chemical Society, 2010 , vol. 132, # 44 p. 15547 - 15549
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 130 °C / Inert atmosphere 2: N-bromosuccinmide / chloroform / 15 h / 20 °C / Darkness; Inert atmosphere View Scheme
参考文献
Hablot, Delphine; Islam, Ashraful; Han, Liyuan; Ziessel, Raymond
Collection of Czechoslovak Chemical Communications, 2012 , vol. 77, # 6 p. 462 - 469
反应条件
1.1: anhydrous iron chloride; sodium / 1 h / 130 °C / Inert atmosphere 1.2: 3 h / 130 °C / Inert atmosphere 2.1: potassium carbonate / N,N-dimethyl-formamide / 130 °C / Inert atmosphere 3.1: N-bromosuccinmide / chloroform / 15 h / 20 °C / Darkness; Inert atmosphere View Scheme
参考文献
Ripaud, Emilie; Demeter, Dora; Rousseau, Theodulf; Boucard-Cetol, Emmanuel; Allain, Magali; Po, Riccardo; Leriche, Philippe; Roncali, Jean
Dyes and Pigments, 2012 , vol. 95, # 1 p. 126 - 133
