1,1,3,3,5,5,7,7-八甲基四硅烷合成路线 （共 14 条）
反应条件
trimethylsilyl trifluoromethanesulfonate 24 h;
参考文献
Procter, Ian; Azouani, Sobine Isabelle; Houbrichs, Rolf
Patent: US2007/249502 A1, 2007 ;
Location in patent: Page/Page column 17 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 23.3333 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.00722222 - 1.72222 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.00583333 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0213889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0444444 - 13.8889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
nickel T=20°C; Further byproducts given;
参考文献
Voronkov; Basenko; Gebel'; Chuvashev
Doklady Chemistry, 2003 , vol. 393, # 4-6 p. 289 - 291
反应条件
tetrahydrofuran; lt;Mg2Cl3(THF)4gt;+lt;AlH3Clgt;- 2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Knott, Wilfried
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 5 p. 629 - 634
参考文献
Lebedev,E.P. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, p. 147 - 150,128 - 131
反应条件
lt;Mg2Cl3(THF)4gt;+lt;AlH3Clgt;- 2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Knott, Wilfried
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 5 p. 629 - 634
