1,1,3,3-四乙基-1,3-二甲基二硅氧烷合成路线 （共 9 条）
反应条件
sulfuric acid; ammonium chloride
参考文献
Westermark
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 947,953
反应条件
carbon dioxide; [(1,3-bis(3-tBu-5-Me-2-oxy-benzyl)-4-Me-MeOC6H2]Zr(CH2Ph)2; tris(pentafluorophenyl)-borane in toluene
T=20°C; 29 h;
参考文献
Matsuo, Tsukasa; Kawaguchi, Hiroyuki
Journal of the American Chemical Society, 2006 , vol. 128, # 38 p. 12362 - 12363
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); triethylamine in benzene
T=140°C; P=38000 Torr; 24 h; other reaction time, temperature; Product distribution;
参考文献
Chatani; Shinohara; Ikeda; Murai
Journal of the American Chemical Society, 1997 , vol. 119, # 18 p. 4303 - 4304
反应条件
[(POCOP)Ir(H)(acetone)]+[B(C6F5)4]- in C6D5Cl
T=23°C; P=760.051 Torr; 3.8 h;
参考文献
Park, Sehoon; Bezier, David; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11404 - 11407
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=100°C; 20 h; Pressure (range begins): 30 <unit not given>Yield given. Yields of byproduct given;
参考文献
Koinuma, Hideomi; Kawakami, Fumiaki; Kato, Hirohiko; Hirai, Hidefumi
Journal of the Chemical Society, Chemical Communications, 1981 , # 5 p. 213 - 214
反应条件
1: NH3
2: diethyl ether; aqueous HCl
3: aqueous HCl
View Scheme
参考文献
Schostakowskii et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 622
p. 593
反应条件
1: diethyl ether; aqueous HCl
2: aqueous HCl
View Scheme
参考文献
Schostakowskii et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 622
p. 593
参考文献
Orlow; Dolgow
Doklady Akademii Nauk SSSR, 1959 , vol. 125, p. 817
Doklady Chemistry, 124-129 <1959> 266
反应条件
200 deg C; water
thermal rearrangement, various substrates; Product distributionMechanism;
参考文献
Zakharov; Molchanova; Shcherbina; Petrovskii; Kabachnik
Russian Chemical Bulletin, 1998 , vol. 47, # 9 p. 1718 - 1724
