4,4'-二硝基二苯二硫醚合成路线 （共 219 条）
反应条件
1: 68 percent / Na2HPO4; HOCH2SO2Na / dimethylformamide; H2O / 2.5 h / 20 °C / 9000.9 Torr
2: 98 percent / iron; hydrochloric acid / H2O / 1 h / 90 °C
3: 96 percent / trichloroisocyanuric acid; [Bmim]BF4; H2O / 0.08 h / 20 °C
View Scheme
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 636 - 640
反应条件
copper(I) sulphide; iron; potassium carbonate; dimethyl sulfoxide
T=110°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Wang, Huifeng; Jiang, Linlin; Chen, Tao; Li, Yarning
European Journal of Organic Chemistry, 2010 , # 12 p. 2324 - 2329
反应条件
in chloroform
T=20°C; 20 h;
参考文献
Mukaiyama, Teruaki; Ikegai, Kazuhiro
Chemistry Letters, 2004 , vol. 33, # 11 p. 1522 - 1523
反应条件
tetrabutyl-ammonium chloride in benzene
1.) reflux, 15 min, 2.) 20 deg C, 4 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
反应条件
tetraethylammonium bromide in benzene
参考文献
Borovikova,G.S. et al.
Zhurnal Organicheskoi Khimii, 1979 , vol. 15, p. 479 - 485,424 - 429
反应条件
1: in dimethyl sulfoxide
T=20°C; 192 h;
2: With hydrogenchloride in water; dimethyl sulfoxide
参考文献
Langler, Richard Francis; Baerlocher, Felix J; Penn, Linda Z
Patent: US2003/220524 A1, 2003 ;
Location in patent: Page/Page column 26 ;
反应条件
sodium thiomethoxide in dimethyl sulfoxide
T=20°C; Substitution; 192 h;
参考文献
Baerlocher, Felix Jakob; Baerlocher, Mark Otto; Langler, Richard Francis; MacQuarrie, Stephanie Lee; Marchand, Maurice Emile
Australian Journal of Chemistry, 2000 , vol. 53, # 1 p. 1 - 5
反应条件
(i) Cl2, (ii) /BRN= 956570/; Multistep reaction;
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
反应条件
sodium hydroxide; sodium hydrogensulfide in ethanol
2.5 h; Heating;
参考文献
Yuferov, A. M.; Akkuratova, O. L.; Sergeev, V. A.; Nedel'kin, V. I.; Yuferov, E. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2560 - 2562
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2794 - 2797
